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Beilstein J. Nanotechnol. 2020, 11, 1789–1800, doi:10.3762/bjnano.11.161
Figure 1: Thermogravimetric analysis (TGA) and 1st derivative DTG of (a) Pt(CO)2Cl2 and (b) Pt(CO)2Br2.
Figure 2: Isothermal TGA traces plotted as a function of temperature and time for (a,b) Pt(CO)2Cl2 and (c,d) ...
Figure 3: Chamber pressure after opening and closing the GIS valve containing a) Pt(CO)2Cl2 and b) MeCpPtMe3.
Figure 4: Pillars deposited at 38 pA. a) 35° tilt image of pillars deposited from top to bottom and from left...
Figure 5: Pillar height a) and volume b) as functions of the electron dose (total number of incident electron...
Figure 6: Comparison of pillars grown in experiment 2 from all three precursors a) and d) MeCpPtMe3, b) and e...
Figure 7: Pillar height a) and volume b) as functions of the number of electrons deposited at 38 pA from MeCp...
Beilstein J. Nanotechnol. 2017, 8, 2410–2424, doi:10.3762/bjnano.8.240
Figure 1: (a) Representative FEBID deposit created from cis-Pt(CO)2Cl2. Representative AES and EDS of “as-dep...
Figure 2: (a) SEM image of a deposit created from cis-Pt(CO)2Cl2, and (b) corresponding EDS spectrum. (c) SEM...
Figure 3: (a) PtCl2 deposit created from cis-Pt(CO)2Cl2; (b) corresponding EDS analysis. (c) SEM image of the...
Figure 4: (a) SEM image of a PtCl2 deposit created from cis-Pt(CO)2Cl2, without any EDS analysis and prior to...
Figure 5: SEM images of a deposit created from cis-Pt(CO)2Cl2: (a) prior to any treatment, and after (b) 48, ...
Figure 6: AES for a deposit created from cis-Pt(CO)2Cl2 (top spectrum) and then subjected to alternating trea...
Figure 7: AFM data for nanostructures created from MeCpPtMe3 using different total exposure times (TET) (per ...
Figure 8: (a) Height of nanostructures created from MeCpPtMe3 as determined by AFM: as-deposited (black bar) ...
Scheme 1: Hess cycle for electron purification of PtCl2. ∆H = −∆Hf PtCl2 + Cl2 bond dissociation enthalpy (BD...
Scheme 2: Hess cycle for atomic hydrogen purification of PtCl2. ∆H = −∆Hf PtCl2 + H2 bond dissociation enthal...